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NEOMYCIN SULPHATE CREAM USP

Posted on August 19, 2020May 24, 2023 By ABHA

NEOMYCIN SULPHATE CREAM USP

PURPOSE:  This Master formula record (MFR) is written to describe the formulae, manufacturing procedure, specifications, packing details of dosage form.

SCOPE: This MFR is performed and is applied during the manufacturing of dosage form.

RESPONSIBILITY / ACCOUNTABILITY: It is the responsibility of Manufacturing Chemist to follow and adhere to this SOP. The Production Pharmacist, QC/QA Manager  are accountable for the strict adherence to the master formula.

COPY ISSUED TO:

Master Copy : Manager Quality Assurance

Copy No. 1 : Production Pharmacist

Copy No. 2 : Manager Quality Control

Copy No. 3 : Ointment Section

PRODUCT NAME: NEOMYCIN SULPHATE CREAMBATCH SIZE:  500 Kg
PRODUCT REFERENCE CODE: UNIT SIZE:  30 g
GENERIC NAME: NEOMYCIN SULPHATE CREAM U.S.P.PACK SIZE:  30 ´ 12 ´ 30 g
DOSAGE FORM: OINTMENTSTRENGTH: N.A.
DEPARTMENT:  OINTMENT DEPARTMENTEXPIRY DATE: AFTER 36 MONTHS FROM THE DATE OF MANUFACTURING

COMPOSITION:

Neomycin SulphateU.S.P.0.5% w/w

EQUIPMENTS TO BE USED:

SR. NO.NAME OF EQUIPMENTASSEMBLING

AS PER SOP NO.

CLEANING

AS PER SOP NO.

1Wax Vessel
2Water Vessel
3Mixing Vessel
4Storage Container (500 Kg)
5Semiautomatic Aluminium Tube Filling & Crimping Machine

RAW MATERIALS:-

S.NO.INGREDIENTS STDTheoretical Quantity Req.Overages %Total Quantity Used
1CM – 1000B.P.16.66616.666 KG
2CETOCETYL ALCOHOLB.P.50.00050.000 KG
3EDTAB.P.0.2500.250 KG
4LIQUID PARAFFIN LIGHTB.P.25.00025.000 KG
5METHYL PARABEN SODIUMB.P.0.2500.250 KG
6NEOMYCIN SULPHATEU.S.P.2.50020.003.000 KG
7PROPYL PRABEN BI SODIUMB.P.1.0001.000 KG
8SODIUM META BISULPHITEB.P.1.6701.670 KG
9WHITE PETROLEUM JELLYB.P.80.00080.000 KG

PACKING MATERIALS:-

S.NO.NAME OF THE MATERIAL THEORETICAL QUANTITY REQ.FOR

RECORD

TOTAL QUANTITY USED
1ADHESIVE TAPE ROLL BROWN1.0001.000 NOS
2CELLO TAPE3.0003.000 NOS
3 TUBE – 30 G16666.00016666.000 NOS
4UNIT CARTON16666.0003.00016669.000 NOS
5OUTER CARTON1388.0002.0001388.000 NOS
6CORRUGATED BOX46.00046.000 NOS

MANUFACTURING SPECIFICATIONS:

Average fill of each Tube is 30 grams.

Wight variation limit allowed in each filled Tube is + 200 mgs.

Melt the waxes at the maintained temperature 70˚ C.

Use accurate weighed quantity of water to make up the final weight of cream.

The temperature of primary area should not be more than 30˚C.

Yield:

Theoretical Yield is 16666 Tubes.

Expected Practical Yield is 16666 + 2% Tube.

 Packing Details:

Transfer the cream from storage tank to Semiautomatic Aluminium Tube Filling & Crimping Machine and start filling and then Crimping of the tubes as per its SOP .

Pack the filled tubes in unit carton.

Pack such 12 tubes in each outer carton.

Seal the outer carton with cello tape.

Pack the 30 outer cartons in specified corrugated  box to give a pack size of 30 x 12 x 30g Tubes.

Seal the each corrugated box with adhesive tape and label it properly by affixing the specified label.

MANUFACTURING PROCESS:

Melt 16.666 kgs of Ceto Macrogol- 1000, 50 kgs of Cetocetyl Alcohol, 25.0 kgs of Liquid Paraffin and 80 kgs White Petroleum Jelly in a Steam Heat Wax Melting Vessel by operating it as per its SOP at temperature 700

Heat 323.00 kg of water at 70°C in Water Vessel by operating it as per its SOP.

Filter and transfer the melted base through Stainless Steel Sieve no. 100 to the mixing vessel and start the machine as per its SOP.

Dissolve 0.250 kg of Methyl Paraben Sodium in 4kg of water and transfer it to the bulk batch.

Dissolve 1.000 kg of Propyl Paraben Sodium in 2kg of water and transfer it to the bulk batch.

Dissolve 0.250 kg of Ethylene Diamine-Tetra Acetic acid in 2kg of water and transfer it to the bulk batch.

Dissolve 1.670kg of Sodium Meta-bisulphite in 5kg of water and transfer it to the bulk batch.

Slowly add rest of the water to bulk batch by saving 10kg of water.

Cool the cream to the room temperature by running the water in the jacket of mixing vessel.

Dissolve 3.0 kg of Neomycin Sulphate in 10kg of hot water and add to the bulk batch.

Mix the whole batch for 90 minutes while running the water in the jacket.

Send the sample to Quality Control Department for bulk testing.

After getting QC Approval, transfer the cream to storage tank.

IN-PROCESS CONTROLS:

The following in-process controls should be maintained during the processing:

Check Raw materials used for manufacturing purpose are all approved materials and have ‘Released’ labels fixed on it.

All weighed Raw materials should be counter-checked by  Manufacturing Chemist. If any discrepancy is noticed, it should be immediately brought to the notice of Production Pharmacist and QC/QA Manager.

Physical characteristics of Raw material like colour, odour, and consistency are checked before compounding.

The total weight of bulk ointment / cream should be checked in the presence of  Manufacturing Chemist and record the same in Batch Manufacturing Record.

pH of the bulk should be checked and it should be with in specified limits.

Bulk sample should be sent for analysis to Quality Control Department before starting the filling and sealing stage.

While the tube filling operation is on, the Manufacturing Chemist should check weight of net filled quantity per tube at the interval of 30 minutes by checking the tare weight of empty tube and gross weight of the filled tube. Record for the same should be kept in Batch Manufacturing Record.

The ‘fill weight’ of ointment or cream per tube should not be less than the labelled amount.

Limit for Weight Variation: Weight claimed on the carton + 200 mg

Manufacturing Chemist will also ensure that the crimping of the filled Aluminium tubes, sealing of plastic tubes is appropriate and embossing of batch number and manufacturing date is conspicuous. Also the quality of embossing will be controlled by adjusting pressure exerted by the jaws, so that pinholes are not developed on the embossed letters / numbers.

The inner and outer cartons should be checked thoroughly for proper batch coding.

Manufacturing Chemist and Production Pharmacist should randomly check that the correct no. of inner cartons are being packed in each outer cartons and also the correct number of outer cartons in each shipper is exactly the same as that shown in proof.

Intimation should be sent to Quality Control Department for finished product sampling and testing.

After the completion of filling and packaging, the coded cartons should be accounted for and rejected printed material should be destroyed in the presence of QC/QA Manager. Maintain the destruction of the same in the Batch Manufacturing Record.

It will be ensure that filling or packaging equipment has been properly cleaned.

Filling or packaging of next product should be commenced only after getting the ‘Line Clearance’ of the previous product, from the IPQA.

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Recent Jobs

Bliss GVS Pharma Ltd-Vacancies for M.Pharm, B.Pharm, MSc in QA, QC, Production Apply

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Zydus Lifesciences -Walk In Interview on 19th March 2025

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Ipca -Walk In Interview For QA/ QC and Maintenance Dept on 23/03/2025

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Torrent Pharma-Walk In Drive for M.Pharm, MSc as ADL Executive on 23rd MARCH, 2025

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Gufic Biosciences-walk in for B.Pharm, MSc, BSc in Quality Control, Production on 22/03/2025 

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Intas- Walk In Interview For Fresher on 22nd March 2025 

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Indeed Jobs-Symed Labs Ltd (Viyash Life Sciences) – Walk-In Drive for Quality Control / Quality Assurance / EHS / ETP on 17th-21st Dec’ 2024

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Indeed Jobs- Siflon Drugs & Pharmaceuticals Pvt. Ltd -Interview on 17th & 18th Dec’ 2024

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Indeed Jobs SRF- Walk In Interview For Multiple Openings on 17th December 2024

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Indeed Jobs Bafna Pharmaceuticals Walk-In Interview on 22nd December 2024.

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